UGC Approved Journal no 63975(19)
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ISSN: 2349-5162 | ESTD Year : 2014
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Published in:

Volume 6 Issue 3
March-2019
eISSN: 2349-5162

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Published Paper ID:
JETIR1903444


Registration ID:
200120

Page Number

289-294

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Title

XANES and EXAFS Studies of Copper(II) Complexes of 1,4-Dihydrquinoxaline -2,3-dione

Abstract

Two copper (II) complexes of 1,4-Dihydrquinoxaline -2,3- dione have been prepared. The two complexes are [Cu(CL)2.2H2O]-L and [Cu(SO4)2.7H2O]-L where L = 1,4-Dihydrquinoxaline -2,3- dione . The ligand 1,4-Dihydrquinoxaline -2,3- dione has been preapared by mixing o-phnylenediamine and oxalic acid dihydrate . Synchrotron radiation source which is available at RRCAT(Raja Ramanna Center for Advance Technology ), Indore, M.P, India has been used for recording the X-ray k-Absorption Near Edge (XANES)and Extended X-ray K-Absorption Fine Structural (EXAFS) spectra of copper(II) complexes. Various X-ray absorption parameters e.g., chemical shift, edge-width and shift of the principal absorption maximum have been obtained with the help of XANES spectra. The EXAFS data obtained has been used to determine the bond length by using four different methods, i.e., Levy’s, Lytle, Lytle, Sayers and Stern’s (LSS) and Fourier transformation methods. Data analysis program Athena and the computer software Origin 6.0 professional have been used to processed the obtained data. The results of the study have been reported in this paper

Key Words

Mixed ligand Copper(II) complexes,RRCAT, XANES, EXAFS,LSS, Athena, , Origin 6.0 professional

Cite This Article

"XANES and EXAFS Studies of Copper(II) Complexes of 1,4-Dihydrquinoxaline -2,3-dione", International Journal of Emerging Technologies and Innovative Research (www.jetir.org), ISSN:2349-5162, Vol.6, Issue 3, page no.289-294, March-2019, Available :http://www.jetir.org/papers/JETIR1903444.pdf

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2349-5162 | Impact Factor 7.95 Calculate by Google Scholar

An International Scholarly Open Access Journal, Peer-Reviewed, Refereed Journal Impact Factor 7.95 Calculate by Google Scholar and Semantic Scholar | AI-Powered Research Tool, Multidisciplinary, Monthly, Multilanguage Journal Indexing in All Major Database & Metadata, Citation Generator

Cite This Article

"XANES and EXAFS Studies of Copper(II) Complexes of 1,4-Dihydrquinoxaline -2,3-dione", International Journal of Emerging Technologies and Innovative Research (www.jetir.org | UGC and issn Approved), ISSN:2349-5162, Vol.6, Issue 3, page no. pp289-294, March-2019, Available at : http://www.jetir.org/papers/JETIR1903444.pdf

Publication Details

Published Paper ID: JETIR1903444
Registration ID: 200120
Published In: Volume 6 | Issue 3 | Year March-2019
DOI (Digital Object Identifier):
Page No: 289-294
Country: Osmanabad, Maharashtra, India .
Area: Physics
ISSN Number: 2349-5162
Publisher: IJ Publication


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